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fifteen) Very careful decant this solution through the flask into your 500mL measuring cylinder. Because the non-polar solvent layer is on top, nearly all It'll be poured into the cylinder.
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19) Position the rectangular Pyrex dish Along with the solvent in the freezer. Ensure the lid is locked in. In case your dish doesn't come with a locking lid, then wrap the opening of the dish with cling movie and put all the dish into a sizable zip lock bag.